Making —Magenta watercolour paint

Ingredients

Current procedure — last updated 18. August 2022

  1. Mix the watercolour paste
    1. Wear a mask. Go outdoors - this can be very messy.
      Pour the medium into the stainless steel container first.
    2. Measure out the powdered pigment.
      Add about a third of it to the Blender Ball, and then top off with about 250ml of medium.
      Seal it up and shake back and forth 60 times.
      Repeat twice more, and then pour in the remaining medium and shake to roughly rinse.
    3. Start dispersing, using a dispersion disc in a drill press.
    4. Cover the bowl while dispersing to limit the dust.
  2. Mill the paste
    1. Set both rollers to 6mil.
    2. Prepare a large bowl and a hopper to use. Find a stand to raise up the bowl to catch the paint to reduce splashing.
    3. Use a nail brush and water to clean the rollers at the end of the first runs.
    4. Put through the mill 8 times.
    5. Test for grind at the end of run #4, #6, and #8.
    6. At the start of run #7, add one drop of clove oil for 250ml of total medium (100ml mix = 4-5 drops) Add the oil to the paste on the slow rollers, rather than in a bowl on in the hopper.
  3. Package into pans
    1. Arrange the 350ish empty 2ml half-pans into rows on a cookie sheet
    2. Fill the pans to the top with a pipette set to 2.3ml
    3. Allow to dry, and then top off
    4. Allow to dry, and then package into wax paper bags

Drapak’s manufacturing notes

18-22. September 2023 - 1 runs @ 150g pigment: 1000ml medium
Pr122 powdered magenta pigment: 150 grams × $0.232/g = $34.80
Watercolour medium 1000ml × $27.71/1000ml = $27.71
Number of new pans filled 117 pans × $0.08/pan Cost of pans = $9.36
Total for materials = $71.87 Material cost/pan = $0.21
Time to mix 20 minutes
Time for pre-dispersion 10 minutes
Time to mill 110 minutes
Time to dispense 120 minutes
Total time 260 minutes
Number of runs 12
Final grind size 7.5-12.5µm
Time spent per pan 0.77 minutes × labour rate $0.48/min= $0.37
Total cost/pan = $0.59

I went back to the previous recipe. That was rough.

The milling was fine, but slow. This stuff is pretty viscous. The dispensing was painfully slow, and finishing the dispensing robot will be a big plus.

All of these were first fills, so it may be more expensive than normal. I will need to do another run in order to have fully filled pans to distribute.

28.-29. August 2023 - 2 runs @ 150g pigment: 1000ml medium
Pr122 powdered magenta pigment: 300 grams × $0.232/g = $84.00
Watercolour medium 2000ml × $27.71/1000ml = $55.42
Number of pans filled 1175 pans × $0.08/pan Cost of pans = $94.00
Total for materials = $233.42 Material cost/pan = $0.30
Time to mix 20 minutes
Time for pre-dispersion 10 minutes
Time to mill 230 minutes
Time to dispense 210 minutes
Total time 470 minutes
Number of runs 13
Final grind size 7.5-12.5µm
Time spent per pan 0.6 minutes × labour rate $0.48/min= $0.29
Total cost/pan = $0.59

I went back to the previous recipe. That was rough.

The milling was fine, but slow. This stuff is pretty viscous. The dispensing was painfully slow, and finishing the dispensing robot will be a big plus.

All of these were first fills, so it may be more expensive than normal. I will need to do another run in order to have fully filled pans to distribute.

17-18. August 2023 - 2 batches of 150g pigment: 1000ml medium
Pr122 powdered magenta pigment: 300 grams × $0.280/g = $84.00
Watercolour medium 1000ml × $25.41/1000ml = $50.82
Number of new pans filled 631 pans × $0.08/pan Cost of pans = $50.48
Total for materials = $185.30 Material cost/pan = $0.15
Time to mix 30 minutes
Time for pre-dispersion 10 minutes
Time to mill 270 minutes
Time to dispense 270 minutes
Total time 280 minutes
Number of runs 12/13
Final grind size 10-12.5µm
Time spent per pan 0.46 minutes × labour rate $0.48/min= $0.22
Total cost/pan = $0.37

This was pretty reasonable, although towards the end, my back was killing me.

Things to note:

Dispensing was miserable. My poor back. Again, the second batch was more viscous, so it took much longer. I have to make a new robot! Like now!

Update! A weekish later: mould appears on the magenta! Remember how honey is an antifungal agent? Well, it turns out that reducing the honey was a profoundly dumb idea. Don't do this! Expensive mistake!

30. August 2022 - 1 batch of 150g pigment: 1000ml medium
Pr122 powdered magenta pigment: 150 grams × $0.232/g = $52.35
Watercolour medium 1000ml × $23.09/1000ml = $23.09
Number of pans filled 393 pans × $0.08/pan Cost of pans = $31.44
Total for materials = $106.88 Material cost/pan = $0.272
Time to mix 22 minutes
Time for pre-dispersion 30 minutes
Time to mill 300 minutes
Time to dispense 100 minutes
Total time 452 minutes
Number of runs 12
Final grind size 10-15µm
Time spent per pan 1.15 minutes × labour rate $0.445/min= $0.511
Total cost/pan = $0.783

This took forever, but it also worked very very well. Mixing was reasonable, and was not as messy as I remembered. I still did it outside, though.

I had less time on the drill press for pre-dispersion mixing, and I think that may have cost me an extra run. All told, I did 12 runs with the magenta, and the extra time milling was worth it. There was much less of the darker grey granules that plague the purple and the magenta when milled less.

I did add the extra water when I began, but around the eighth run, I needed to add even more in order to keep it fluid. This stuff really sucks up water.

Dispensing was miserable. Partly this was because I had rejigged my schmoo dispenser to use a new quieter stepper drive and I had not calibrated it properly. However, the magenta is also very very thick, and took longer to squeeze through the tubes.

17-18. August 2022 - 2 batches of 150g pigment:1000ml medium
Pr122 powdered magenta pigment: 2 x 150 grams × $0.349/g = $104.70
Watercolour medium 1000ml × $23.09/1000ml = $46.18
Number of pans filled 700 pans × $0.08/pan Cost of pans = $56.00
Total for materials = $206.88 Material cost/pan = $0.2296
Time to mix 15 minutes
Time for pre-dispersion 30 minutes
Time to mill 345 minutes
Time to dispense 150 minutes
Total time 540 minutes
Final grind size 10-15µm
Time spent per pan 0.77 minutes × labour rate $0.445/min= $0.343
Total cost/pan = $0.573

This was much better than milling the violet!

I mixed the pigment in the shaker bottles. I measured out 75g of pigment and scooped it into the bottle. Then I added about 330ml of medium and shook for 45-60s. Then I repeated this, and rinsed the bottle with the remaining medium. Making a paper funnel to place inside the bottle to guide the pigment and hold down the dust might be nice.

The shaker bottles left quite a foamy mixture, so pre-dispersing on the drill press helped get a more homogenous mixture.

Milling was pretty straight forward. On the first batch, run #3 was very slow. This was because I had not been stirring the mix in the funnel and in the catch bowl in order to keep things consistent. On the second batch, I consistently mixed the batch in the hopper and the catch bowl and it went about 30min faster.

I added the clove oil earlier on the second run. This seemed to make a more consistent batch, but I woke up in the night with nasty allergies. Nasty!

Dispensing took a loooong time. As usual. I need to get that electronic dispenser going properly.

I should note that the magenta seemed to swell and take on water a little, a little like the yellow pigment. During the first batch, this slowed things down quite a bit. I added 125ml of water to the mix for the second batch, and this sped things up quite a bit.

It is interesting that the cost of the pigment is still less of a factor than the labour.

20. July 2022 — 3 cups total using 1:2 from Kama Dispersion
Pr122 dispersed magenta pigment: 250ml = $81.13
Watercolour medium 2 cups × $11.86/4 cups = $5.93
Number of pans filled 300 pans × $0.08/pan Cost of pans = $24.00
Total for materials = $111.06 Material cost/pan = $0.370
Time to mix 15 minutes
Time for pre-dispersion 0 minutes
Time to mill 105 minutes
Time to dispense 40 minutes
Total time 160 minutes
Final grind size 10-15µm
Time spent per pan 0.53 minutes × labour rate $0.445/min= $0.237
Total cost/pan = $0.607

I found a 250ml bottle of Kama Pigments magenta magenta Aqua Dispersion. I mixed it into 500ml of watercolour medium with a whisk.

The milling was pretty good. There was a small amount that made it through the rollers, but otherwise the settings seemed good. It could be worth seeing if the rollers could be a little tighter.

I made 8 runs through the mill.

After the fourth run, I tested the grind and found that it was already excellent.

Clean up was great, and dispensing went quickly. I used a pipette set to 2.2ml and the dispensing went fast!

As a postscript, as the mix dried in the pans, the amount magenta was less than expected. I recommend using a 1:1 mix of medium to pigment dispersion if I mix this from the dispersions in the future.

16. March 2022 — 3 cups total using 1:2 from Kama Dispersion

750mL of Magenta Pr122 ($6.06 of medium + $80.13 of dispersion) = $86.19/368 pans = $0.234 per pan

Well, this is embarrassing to admit, but I have been milling a different pigment than I normally use. I bought the magenta pigment recommended by handprint.org, Quinacridone Violet (PV19), instead of Quinacridone Magenta (PR122). I have been losing sleep and going crazy trying to get magenta out of violet! This was actually a relief, since I was quite upset to be unable to get magenta, and I was worried that the problem was my competence. I am still concerned that the pigment is somewhat granular, but further experiments will help with this. I started to dispense the violet into pans: it was so smooth and creamy in comparison to the pre-made dispersions I bought.

Speaking of which, I did find an older bottle of Kama magenta dispersion to use for next semester. I made a batch of medium to mix it with, and then poured it into pans. The magenta was a little bit lumpy compared to the creaminess of the violet I made, but it is simply a better colour. What a learning experience!

Note: this batch had to be made in a hurry and was not milled.